ISSN 1006-3021 CN11-3474/P
Published bimonthly started in 1979
利用ICP-AES快速检测碳酸盐金属元素的方法研究
  
关键词:geological mine  limestone  CaO  major and minor elements  ICP
基金项目:国家自然科学基金面上项目(编号: 41473061);中国地质调查局地质调查项目(编号: 121201103000150011)
作者单位E-mail
宋晓红 岛津企业管理(中国)有限公司 北京分析中心 fxsxh@shimadzu.com.cn 
刘建华 中国地质科学院矿产资源研究所, 国土资源部盐湖资源与环境重点实验室 1844041600@qq.com 
乜贞 中国地质科学院矿产资源研究所, 国土资源部盐湖资源与环境重点实验室  
冯旭 岛津企业管理(中国)有限公司 北京分析中心  
杨桂香 岛津企业管理(中国)有限公司 北京分析中心  
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摘要:
Quick Determination of CaO and Other Major and Minor Elements in Limestone by ICP-AES
      In this paper, CaO up to 54% and other major and minor elements in limestone (GBW03105a ) certified reference material using wet digestion were determined with the method of combining internal standard and matrix matching by ICP-AES. Sample recoveries and dilution rates were respectively processed to test minor elements and high content elements. The results were satisfactory with recoveries of 94%~108%, dilution rates of 99.4%~100.2% and stability low 4% (n=6). Experiment data were in very good agreement with certified values. This method was adopted to the analysis of limestone sample in geological survey with the advantages of simple operation, high accuracy, precision and repeatability.
SONG Xiao-hong,LIU Jian-hua,NIE Zhen,FENG Xu,YANG Gui-xiang.2016.Quick Determination of CaO and Other Major and Minor Elements in Limestone by ICP-AES[J].Acta Geoscientica Sinica,37(6):763-768.
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