利用ICP-AES快速检测碳酸盐金属元素的方法研究 |
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关键词:geological mine limestone CaO major and minor elements ICP |
基金项目:国家自然科学基金面上项目(编号: 41473061);中国地质调查局地质调查项目(编号: 121201103000150011) |
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摘要: |
Quick Determination of CaO and Other Major and Minor Elements in Limestone by ICP-AES |
In this paper, CaO up to 54% and other major and minor elements in limestone (GBW03105a ) certified reference material using wet digestion were determined with the method of combining internal standard and matrix matching by ICP-AES. Sample recoveries and dilution rates were respectively processed to test minor elements and high content elements. The results were satisfactory with recoveries of 94%~108%, dilution rates of 99.4%~100.2% and stability low 4% (n=6). Experiment data were in very good agreement with certified values. This method was adopted to the analysis of limestone sample in geological survey with the advantages of simple operation, high accuracy, precision and repeatability. |
SONG Xiao-hong,LIU Jian-hua,NIE Zhen,FENG Xu,YANG Gui-xiang.2016.Quick Determination of CaO and Other Major and Minor Elements in Limestone by ICP-AES[J].Acta Geoscientica Sinica,37(6):763-768. |
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