太平洋多金属结核及沉积物标准物质研制 |
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关键词:reference material polymetallic nodule deep-sea sediment |
基金项目:中国大洋协会“八五”综合研究课题 |
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摘要: |
The Collaborative Study on Geochemical Reference Materials of Pacific Polymetallic Nodules and Sediments |
The collaborative study on the geochemical reference materials of two polymetallic nodules(GSPN_2 and GSPN_3) and two marine sediments(GSMS_2 and GSMS_3) has been completed. The raw materials of GSPN_2, GSPN_3, GSMS_2 and GSMS_3 were collected from the Pacific CC(clarion_clipperton) zone and the central_Pacific basin(CP zone) respectively. The selected materials were processed to be homogeneous powder(size<74μm). The homogeneity of prepared samples was tested by X_Ray Fluorescence(XRF) method. For all tested elements of 30 subsamples taken in random from a batch, their measurement precision(Relative Standard Divetion, RSD) is better than 0.6%. 32 laboratories, including 18 abroad laboratories participated in the collaborative analysis of the four samples. 79(in GSPN_2 and GSPN-3) and 81(in GSMS_2 and GSMS-3) constituents were determinated, of which 63 were certified. The sums of the contents of constituents determinated for the four samples are 99.7%, 99.5%, 99.8% and 99.7% respectively. The four reference materials, as Certified Reference Materials(CRMs), had been approved by State Bureau of Technical Suppervision in 1997. The serial numbers are GBW07295, GBW07296, GBW07315 and GBW07316 respectively. |
WANG Yi-min,LI Jia-xi,GAO Yu-shu,SONG Hao-wei,LUO Dai-hong,WANG Xiao-hong,CHEN Wei-yue,TENG Yun-ye,ZHOU Shi-guang.1998.The Collaborative Study on Geochemical Reference Materials of Pacific Polymetallic Nodules and Sediments[J].Acta Geoscientica Sinica,19(3):298-307. |
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