ISSN 1006-3021 CN11-3474/P
Published bimonthly started in 1979
原位LA-ICP-MS磷灰石裂变径迹实验流程建立与应用
投稿时间:2023-11-12  修订日期:2024-01-14
关键词:apatite  fission track dating  in-situ LA-ICP-MS method  international reference samples  tectono-thermal evolution
基金项目:国家自然科学基金项目(面上项目,重点项目,重大项目)
作者单位邮编
李晨星 中国石油大学(北京)油气资源与工程全国重点实验室 102249
常健* 中国石油大学(北京)油气资源与工程全国重点实验室 
邱楠生 中国石油大学(北京)油气资源与工程全国重点实验室 
曹世纪 中国石油大学(北京)油气资源与工程全国重点实验室 
张应鳞 中国石油大学(北京)油气资源与工程全国重点实验室 
郑立庆 中国石油大学(北京)油气资源与工程全国重点实验室 
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摘要:
In-situ LA-ICP-MS Apatite Fission Track Experiment Procedure Development and Application
      The in-situ LA-ICP-MS (laser ablation-inductively coupled plasma mass spectrometry) apatite fission track dating technique has gradually become widely used in thermochronology laboratories due to its safety and efficiency advantages. Based on analysis of the principles of the external detector method and the in-situ LA-ICP-MS method, this study has improved the sample preparation procedures for apatite fission track dating and introduced the experimental protocols for in-situ LA-ICP-MS apatite fission track dating established in the thermochronology laboratory of China University of Petroleum (Beijing). Using the newly established testing procedure, the international reference samples Fish Canyon Tuff and Durango were analyzed, yielding ages of 28.70±2.70 Ma (2σ, MSWD=0.63) and 32.01±0.52 Ma (2σ, MSWD=0.91), respectively. These ages are consistent with the recommended ages within the error range. When applying the LA-ICP-MS method to analyze Jurassic samples from the Qianjiadian basin in Yanqing district, 7 apatite fission track ages ranged from 91.18 to 74.28 Ma, which are in good agreement with the results obtained using the external detector method by previous researchers. Through thermal history modeling, it was revealed that the western segment of the Yanshan region experienced two cooling events: 140-130 Ma and 100-0 Ma, since the Jurassic period. This study demonstrates that the newly established in-situ LA-ICP-MS apatite fission track dating experimental procedure in the laboratory is reliable and offers broader application prospects compared to traditional external detector methods.
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